دارویی. اولین کنفرانس ملی علوم و فناوری نانو، یزد، دانشگاه پیام نور یزد، سازمان علمی دانشجویی مهندس برق.
50) Khodabakhshi A, Amin M.M, Mozffari M. (2011). Synthesis of magnetite nanoparticles and evaluation of its efficiency for Arsenic removal from simulated industrial wastewater. Iran.J. Environ. Health. Sci. Eng, Vol 18, No. 3.PP 198-200.
51) Shen Y.F, Tang J, Nie Z.H, wang Y.D, Ren, L. (2009). Preparation and application of magnetic Fe3O4 nanoparticles for wastewater purification. Elsevier 312319.
52)Foca-Nici ciurlica E.l, Nadefde C, Greangaga D.E, carlexcu A and Badescu V. (2010). Antibiotic coated magnetic nonoparticles for biological applications. Nanocon.
53) Pal S, Chandra S, Phan M-H, Mukhjee P and srikanth H. (2009). Carbon nonostraws: nanotubes filled with super paramagnetic nonoparticles. Nanotechnology 485604 .pp7.
54)Nguyen Hoang HAI, Nguyen Chau and Nguyen Hoang Luong. (2008). Applications of magnetite nanoparticles for water treatment and for DNA and cel Sepration. Journal of the Korean physical society. vol. 53, No 3. PP 1601-1606.
55) Mahdavi M, Bin Ahmadi M, Jelas Haron Md, Namvar F, Nadi B, Zaki Ab Rahman M and Amin J. (2013). Synthesis, surface modification and characterisation of biocompatible magnetic iron oxide nanoparticles for biomedical applications. Molecules. 18, 7533- 7548.
56) C. Shundo, H. Zhang, T. Nakanishi, T. Osaka; Colloids and Surfaces B: Bio interfaces 97 (2012), 221-225.
57) Z. Zhu, O. Rezhdo, M. Perrone, Z. Bao, A. Munir, J. Wang, H. Zhou, J. Shao; Colloids and Surfaces B: Biointerfaces 102 (2013), 428-434.
58) اثنا عشری ایوری حسین، عربی هادی. (1392). سنتز نانو ذرات مغناطیسی اکسید آهن به روش همرسوبی و بررسی تأثیر نسبت غلظت مواد واکنش دهنده بر اندازه و خواص مغناطیسی ذرات. علم و مهندسی سرامیک. جلد 2 شماره 1.
59) Ghandoor H.El, Zidan H.H , Mostafa M.H. Khalili and Ismail M.I.M. (2012). Synthesis and some physical properties of magnetic (Fe3O4) nanoparticles. Internaional Journal of electro chemical science. 7.5734-5745.
60) L. Cabrera, S. Gutierrez, N. Menendez. M. P. Morales, P. Herrasti; Electrochimica Acta 53 (2008), 3436-3441.
61) Al. Priola, A. Gianni, R. Bongiovanni, S. G. Starodubtsev, S. Abramchuch, S. N. Polyakov, V. V. Volkov, E. V. Schtykova, K. A. Dembo; Europen Polymer Journal 46 (2010), 2105-2111.
62) بهرامی محمد، برومند نسب سعید، کشکولی حیدرعلی، فرخیان فیروزی احمد، بابایی علی اکبر. (1392). سنتز نانوذرات Fe3O4 و بررسی کارایی آن در حذف کادمیم از محلول آبی. آب و فاضلاب شماره 3.
63) بهمنی منوچهر، عباسی لاله، فرجی محمد. (1392). سنتز نانوذرات مغناطیسی Fe3O4 و کاربرد آن برای استخراج و پیش تغلیظ دارواز نمونه های محیطی. مجله علمی- پژوهشی شیمی کاربردی. سال هشتم، شماره 26.
64) G. Marchegiani, P. Imperatori, A. Mari, I. Pilloni, A. Chiolerio, P. Allia, P. Tiberto, L. Suber; Ultrasonic Sonochemistry 19 (2012), 877-882.
65) J. Ding, K. Tao, J. Li, S. Song, K. Sun; Colloids and Surfaces B: Bio interfaces 79 (2010), 184-190.
66) Asan Maryam, Hasanpour Ahmad, niyaifar Mohammad. (1390). Preparation of Fe3O4/ZnO core-shell Nanopowders and comparison of their magnetic and optical properties. PACS. No 81.M.A. Kelly, K.D. Altria, C. Grace, B.J. Clark; Journal of Chromatography A 798 (1998), 297–306
67)Cui Yali, Hui wenli, wang Huirong, wang Lijun, chen chao. Preparation and characterizition of Fe3O4 /Au composite particles.
68) Chunmei Yu, Jianwei Guo, Haiying Gu. (2009). Electro catalytical oxidution of nitrite and it’s determination based on Au/ Fe3O4 nanoparicles. Wiley inter science. No9. 1005-1011.
69) Ma H, Zhou J, coruntu D, Yu M.H, Chen J.F. (2008). Fabrication of magnetic porous hollow silica drug carriers using caco3/ Fe3o4 composite nanoparticles and cationic surfactant double templates. Journal of Applied physics. 103, 07A320.
70) Hangmei L, Jubai L, xia L, Shengxiang J.A. (2009). Novel multiwalded carbon nanotubes bonded fused- silica fiber for solid phase microextraction- gas chromatographic analysis of phenols in water samples, talanta. 78, 229. 935.
71)- امیر ذهنی ملیحه، عامیان آرزو. (1389). ارزیابی نانوتیوپ های کربنی به عنوان جاذب در استخراج با فاز جامد برای استخراج فنل از محلول های آب. نخستین همایش منطقه ای یافته های نوین شیمی و مهندسی شیمی دانشگاه آزاد اسلامی واحد کرمانشاه.
72) Thurman, E.M.Mills; Chemical Analysis 147, Solid Phase extraction Principles, John Willy, Newyork (1998)
73) C. F. Pool, S. L. C. Seiber, T. D. S. Champan; Journal of Chromatography B
689 (1997), 245.
74) B. Barcelo, D.Hennion, analytica chimica acta (1995), 318
75) J. S. First; Analytical Solid Phaseeytraction, 2ndedition, 124 (1999), 19
76) M. Moors, D. L. Massart, R. D. McDowau; Chemisty 66 (1994), 277.
77) Robert L.Grob, Eugene F. Barry. (2004). Modern practices of gas chromatography. Foruth edition. John wiley & sons, Inc..
78) G. L. Lensmeyer, C. Onsager, I. H. Carlson, D. A. Wiebe, Journal of Chromatography A 691 (1995), 259.
79) C. Ponce, L. Pera, L. T. A. Zamora, P. Bueno; Talanta 46 (1998), 1371.
80) D. Dengtsson, S. Ramberg; Journal of Chromatography B33 (1995), 554.
81) G. Rauret; Talanta 46 (1998), 449.
82) D. S. Jesas, M. Carvallho, M. S. Ferreira; Talanta 46 (1998), 152 .
83) Z. Mester, R. Strurgeon, Spectrochimica Acta Part B 60 (2005), 1243-1296.
84 (گلستانه، مهشید، قریشی،سید مهدی، هنرمند، ابراهیم، 1387، روش های فیزیکی و شیمیایی جداسازی گ جلد اول ، انتشارات جاودانه جنگل، صفحه 120-59
85) E. M. Thurman; Solid phase extraction principle and practice8 Willy (1998).
86) D. Harvey; Modern Analytical chemistry, The McGraw-Hill Companies (2000)
Pantoprazole, a proton pump inhibitor drug that is used to control stomach acid. The main role of this drug in the body is acid stable. Determining and measuring the drug in water and wastewater treatment and reducing toxicity in biological fluids is of great importance and identification of a variety of methods have been presented. A solid phase extraction sample preparation technique is useful, fast and simple. In this study, the performance of the modified nanoparticles (Fe3O4) with a cationic surfactant Cetyl trimethyl ammonium bromide (CTAB) as an adsorbent for pantoprazole drug extraction from real samples was analyzed. The parameters affecting the extraction process were investigated and optimized in terms of the drug determined by using UV-visible spectroscopy technique. The parameters affecting the extraction efficiency such as the pH of the solution, the amount of CTAB, extraction time, the amount of adsorbent (Fe3O4), the type and amount of detergent (solvent), desorption time, were studied and optimized. Under optimal conditions, the calibration curve was linear over the concentration ranges of 0.1-1.2 µg/ml for pantaprazole. Proposed method for measuring pantoprazole drug in aqueous samples and human plasma applied and satisfactory results were obtained . All procedures showed that the method for extraction of pantaprazole of real samples, was fast and efficient
Keywords: pantoprazole, solid phase extraction, magnetic nanoparticles (Fe3O4), surfactant (CTAB), Spectrophotometer UV / Vis
Islamic Azad University
Central Tehran Branch
Faculty of Sciences – Department of Chemistry
“M.Sc” Thesis
On Applied Chemistry
Preconcentration and determination of pentaprazole sodium-sesquihydrate in real samples by using Magnetic iron oxide nanoparticles coated Cetyl trimethyl ammonium Bromide
Dr. Elahe Konoz
Valeh Saeedi
winter 2015
1 pantaprazole
2 Protonix
3 Zogliner-Ellison syndrome
4 Omeprezole
6 Rabeprazole
7 Esomeprazole
8 Domperadone
9 Basavaiah
10 Kumar
11 N-Bromosuccinimide
1- Ferrofluid
4- Surface active agent
15 Ionic Surfactant
16 Nonionic Surfactant
17 Amphoteric Surfactant
18 . Microemulesion
19 . Thermal decomposition
20 . Solvothermal
21 . Sonochemical
22 . Microwave assisted
23 . Chemical vapor deposition
24 . Combustion
25. Carbon arc
26 . Laser pyrolysis
27 . Oil/water
28 . Water/oil
29 . Nanoreactor
30 Scanning Probe Microscopy
31 X-Ray Diffraction
32 X-Ray Photoelectron Spectroscopy
33 Transmission Electron Microscopy
34 Scanning Electron Microscopy
35 Scanning Tunneling Microscopy
36 Atomic Force Microscopy
37 Vibration Sample Magnetometer
1-Rohem and Havese
4-Mixed – Made sorbents
1- Magnetic NanoParticles
2- Hemi micelle
47-Ad micelle
1- Limit Of Detection
2- Limit of Quantification
3-Preconcentration Factor
1-Inter-day precision
2-Intra- day precision

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